Gráfico nº 01: Difratometria de raio X da amostra de ... · 46-1409 (I) - Muscovite-2M1, V-Ba-rich - (K,Ba,Na)0.75(Al,Mg,Cr,V)2(Si,Al,V)4O10(OH,O)2 - Y: 54.84 % - d x by: 1. - WL:

Gráfico nº 01: Difratometria de raio X da amostra de cerâmica I002M3T3

(Dr. Fábio Ramos Dias de Andrade – IGc/USP - 2007)

2

46-1409 (I) - Muscovite-2M1, V-Ba-rich - (K,Ba,Na)0.75(Al,Mg,Cr,V)2(Si,Al,V)4O10(OH,O)2 - Y: 54.84 % - d x by: 1. - WL: 1.54056 - Monoclinic - a 5.2099 - b 9.0729 - c 20.0639 - alpha 90.000 - beta 95.715 - gam46-1045 (*) - Quartz, syn - SiO2 - Y: 54.84 % - d x by: 1. - WL: 1.54056 - Hexagonal - a 4.91344 - b 4.91344 - c 5.40524 - alpha 90.000 - beta 90.000 - gamma 120.000 - Primitive - P3221 (154) - 3 - 113.010 - I/Ic PC:\data\ipen\casimiro\loteii\2.RAW - File: 2.RAW - Type: 2Th/Th locked - Start: 3.00 ° - End: 65.00 ° - Step: 0.05 ° - Step time: 1. s - Temp.: 25 °C (Room) - Time Started: 16 s - 2-Theta: 3.00 ° - Theta: 1.50 ° - Phi: 0.

I(cps

)

0

1000

2000

° (2θ)

5 10 20 30 40 50 60

p. 61

Gráfico nº 02: Difratometria de raio X da amostra de cerâmica I002T2M2


1

46-1409 (I) - Muscovite-2M1, V-Ba-rich - (K,Ba,Na)0.75(Al,Mg,Cr,V)2(Si,Al,V)4O10(OH,O)2 - Y: 50.00 % - d x by: 1. - W L: 1.54056 - Monoclinic - a 5.2099 - b 9.0729 - c 20.0639 - alpha 90.000 - beta 95.715 - gam46-1045 (*) - Quartz, syn - SiO2 - Y: 50.00 % - d x by: 1. - WL: 1.54056 - Hexagonal - a 4.91344 - b 4.91344 - c 5.40524 - alpha 90.000 - beta 90.000 - gamma 120.000 - Primitive - P3221 (154) - 3 - 113.010 - I/Ic PC:\data\ipen\casimiro\loteii\1.RAW - File: 1.RAW - Type: 2Th/Th locked - Start: 3.00 ° - End: 65.00 ° - Step: 0.05 ° - Step time: 1. s - Temp.: 25 °C (Room) - T ime Started: 16 s - 2-Theta: 3.00 ° - Theta: 1.50 ° - Phi: 0.

I(cps

)

0

100 0

200 0

° (2θ)

5 10 20 30 40 50 60

p. 62

] Gráfico nº 03: Difratometria de raio X da amostra de cerâmica I002M4T4


3

46-1409 ( I) - Mus covi te-2M1, V-Ba-rich - (K,Ba,N a)0.75(Al ,M g,Cr,V)2(Si,Al,V)4O10(OH ,O)2 - Y: 25.36 % - d x by: 1 . - W L: 1.54056 - M onoclin ic - a 5.2099 - b 9.0729 - c 20.0639 - alpha 90.000 - beta 95.715 - gam46-1045 (*) - Quartz, syn - SiO2 - Y: 25.36 % - d x by: 1. - W L: 1.54056 - Hexagonal - a 4.91344 - b 4.91344 - c 5.40524 - alpha 90.000 - beta 90.000 - gamm a 120.000 - Pr im itive - P3221 (154) - 3 - 113.010 - I/Ic PC:\data\ipen\casim iro\lote ii\3 .RAW - File: 3.R AW - T ype: 2Th/Th lock ed - Start: 3.00 ° - End: 65.00 ° - Step: 0.05 ° - Step tim e: 1. s - Temp.: 25 °C (R oom ) - T im e Started: 16 s - 2-Theta: 3.00 ° - T heta: 1 .50 ° - Phi : 0.

I(cps

)

0

100 0

200 0

300 0

400 0

500 0

° (2θ)

5 10 20 30 40 50 60

p. 63

Gráfico nº 04: Difratometria de raio X da amostra de cerâmica I002M1T4


4

46-1409 (I) - Muscovite-2M1, V-Ba-rich - (K,Ba,Na)0.75(Al,Mg,Cr,V)2(Si,Al,V)4O10(OH,O)2 - Y: 88.48 % - d x by: 1. - W L: 1.54056 - Monoclinic - a 5.2099 - b 9.0729 - c 20.0639 - alpha 90.000 - beta 95.715 - gam46-1045 (*) - Quartz, syn - SiO2 - Y: 88.48 % - d x by: 1. - WL: 1.54056 - Hexagonal - a 4.91344 - b 4.91344 - c 5.40524 - alpha 90.000 - beta 90.000 - gamma 120.000 - Primitive - P3221 (154) - 3 - 113.010 - I/Ic PC:\data\ipen\casimiro\loteii\4.RAW - File: 4.RAW - Type: 2Th/Th locked - Start: 3.00 ° - End: 65.00 ° - Step: 0.05 ° - Step time: 1. s - Temp.: 25 °C (Room) - Time Started: 16 s - 2-Theta: 3.00 ° - Theta: 1.50 ° - Phi: 0.

I(cps

)

0

1000

° (2θ)

5 10 20 30 40 50 60

p. 64

Gráfico nº 05: Difratometria de raio X da amostra de cerâmica I002M2T2 (Dr. Fábio Ramos Dias de Andrade – IGc/USP - 2007)

5

46-1409 (I) - Muscovite-2M1, V-Ba-rich - (K,Ba,Na)0.75(Al,Mg,Cr,V)2(Si,Al,V)4O10(OH,O)2 - Y: 25.50 % - d x by: 1. - W L: 1.54056 - Monoclinic - a 5.2099 - b 9.0729 - c 20.0639 - alpha 90.000 - beta 95.715 - gam46-1045 (*) - Quartz, syn - SiO2 - Y: 25.50 % - d x by: 1. - WL: 1.54056 - Hexagonal - a 4.91344 - b 4.91344 - c 5.40524 - alpha 90.000 - beta 90.000 - gamma 120.000 - Primitive - P3221 (154) - 3 - 113.010 - I/Ic PC:\data\ipen\casimiro\loteii\5.RAW - File: 5.RAW - Type: 2Th/Th locked - Start: 3.00 ° - End: 65.00 ° - Step: 0.05 ° - Step time: 1. s - Temp.: 25 °C (Room) - T ime Started: 16 s - 2-Theta: 3.00 ° - Theta: 1.50 ° - Phi: 0.

I(cps

)

0

100 0

200 0

300 0

400 0

500 0

° (2θ)

5 10 20 30 40 50 60

p. 65

Gráfico nº 06: Difratometria de raio X da amostra de cerâmica I002P1Sup (Dr. Fábio Ramos Dias de Andrade – IGc/USP - 2007)

6

46-1409 (I) - Mus covi te-2M1, V-Ba-rich - (K,Ba,Na)0.75(Al,Mg,Cr,V)2(Si,Al,V)4O10(OH ,O)2 - Y: 57.73 % - d x by: 1. - W L: 1.54056 - Monoclinic - a 5.2099 - b 9.0729 - c 20.0639 - alpha 90.000 - beta 95.715 - gam46-1045 (*) - Quartz, syn - SiO2 - Y: 75.57 % - d x by: 1. - WL: 1.54056 - Hexagonal - a 4.91344 - b 4.91344 - c 5.40524 - alpha 90.000 - beta 90.000 - gamm a 120.000 - Prim itive - P3221 (154) - 3 - 113.010 - I/Ic PC:\data\ipen\casim iro\loteii\6.RAW - File: 6.RAW - Type: 2Th/Th lock ed - Start: 3.00 ° - End: 65.00 ° - Step: 0.05 ° - Step time: 1. s - Temp.: 25 °C (Room) - T ime Started: 16 s - 2-Theta: 3.00 ° - Theta: 1.50 ° - Phi : 0.

I(cps

)

0

100 0

° (2θ)

5 10 20 30 40 50 60

p. 66


7

10-0393 (*) - Albite, disordered - Na(Si3Al)O8 - Y: 50.00 % - d x by: 1. - WL: 1.54056 - Triclinic - a 8.165 - b 12.872 - c 7.111 - alpha 93.45 - beta 116.4 - gamma 90.28 - Base-centred - C-1 (0) - 4 - 667.792 - I/Ic PD31-0966 (*) - Orthoclase - KAlSi3O8 - Y: 12.50 % - d x by: 1. - WL: 1.54056 - Monoclinic - a 8.556 - b 12.98 - c 7.205 - alpha 90.000 - beta 116.01 - gamma 90.000 - Base-centred - C2/m (12) - 4 - 719.122 - I/Ic PDF46-1045 (*) - Quartz, syn - SiO2 - Y: 112.91 % - d x by: 1. - WL: 1.54056 - Hexagonal - a 4.91344 - b 4.91344 - c 5.40524 - alpha 90.000 - beta 90.000 - gamma 120.000 - Primitive - P3221 (154) - 3 - 113.010 - I/Ic C:\data\ipen\casimiro\loteii\7.RAW - File: 7.RAW - Type: 2Th/Th locked - Start: 3.00 ° - End: 65.00 ° - Step: 0.05 ° - Step time: 1. s - Temp.: 25 °C (Room) - Time Started: 16 s - 2-Theta: 3.00 ° - Theta: 1.50 ° - Phi: 0.

I(cps

)

0

1000

° (2θ)

5 10 20 30 40 50 60

p. 67


j1

46-1409 (I) - Muscovite-2M1, V-Ba-rich - (K,Ba,Na)0.75(Al,Mg,Cr,V)2(Si,Al,V)4O10(OH,O)2 - Y: 45.27 % - d x by: 1. - W L: 1.54056 - Monoclinic - a 5.2099 - b 9.0729 - c 20.0639 - alpha 90.000 - beta 95.715 - gam46-1045 (*) - Quartz, syn - SiO2 - Y: 45.27 % - d x by: 1. - WL: 1.54056 - Hexagonal - a 4.91344 - b 4.91344 - c 5.40524 - alpha 90.000 - beta 90.000 - gamma 120.000 - Primitive - P3221 (154) - 3 - 113.010 - I/Ic PC:\data\ipen\casimiro\loteii\t1.RAW - F ile: j1.RAW - Type: 2Th/Th locked - Start: 3.00 ° - End: 65.00 ° - Step: 0.05 ° - Step time: 1. s - Temp.: 25 °C (Room) - T ime Started: 16 s - 2-Theta: 3.00 ° - Theta: 1.50 ° - Phi:

I(cps

)

0

100 0

200 0

° (2θ)

5 10 20 30 40 50 60

p. 68

Gráfico nº 09: Difratometria de raio X da amostra de cerâmica I002Sup (Dr. Fábio Ramos Dias de Andrade – IGc/USP - 2007)

j2

46-1409 (I) - Muscovite-2M1, V-Ba-rich - (K,Ba,Na)0.75(Al,Mg,Cr,V)2(Si,Al,V)4O10(OH,O)2 - Y: 65.69 % - d x by: 1. - WL: 1.54056 - Monoclinic - a 5.2099 - b 9.0729 - c 20.0639 - alpha 90.000 - beta 95.715 - gam46-1045 (*) - Quartz, syn - SiO2 - Y: 65.69 % - d x by: 1. - WL: 1.54056 - Hexagonal - a 4.91344 - b 4.91344 - c 5.40524 - alpha 90.000 - beta 90.000 - gamma 120.000 - Primitive - P3221 (154) - 3 - 113.010 - I/Ic PC:\data\ipen\casimiro\loteII\T2.RAW - File: j2.RAW - Type: 2Th/Th locked - Start: 3.00 ° - End: 65.00 ° - Step: 0.05 ° - Step time: 1. s - Temp.: 25 °C (Room) - Time Started: 16 s - 2-Theta: 3.00 ° - Theta: 1.50 ° - Phi:

I(cps

)

0

1000

2000

° (2θ)

5 10 20 30 40 50 60

p. 69


j3

46-1409 (I) - Mus covi te-2M1, V-Ba-rich - (K,Ba,N a)0.75(Al,M g,Cr,V)2(Si,Al,V)4O10(OH ,O)2 - Y: 28.75 % - d x by: 1. - W L: 1.54056 - M onoclin ic - a 5.2099 - b 9.0729 - c 20.0639 - alpha 90.000 - beta 95.715 - gam46-1045 (*) - Quartz, syn - SiO2 - Y: 28.75 % - d x by: 1. - W L: 1.54056 - Hexagonal - a 4.91344 - b 4.91344 - c 5.40524 - alpha 90.000 - beta 90.000 - gamm a 120.000 - Prim itive - P3221 (154) - 3 - 113.010 - I/Ic PC:\data\ipen\casim iro\loteII\t3.RAW - F ile: j3.RAW - T ype: 2Th/T h loc ked - Start: 3.00 ° - End: 65.00 ° - Step: 0.05 ° - Step tim e: 1. s - Tem p.: 25 ° C (R oom ) - T im e Started: 16 s - 2-T heta: 3.00 ° - T heta: 1.50 ° - Phi :

I(cps

)

0

100 0

200 0

300 0

400 0

° (2θ)

5 10 20 30 40 50 60

p. 70

Gráfico nº 11: Difratometria de raio X da amostra de cerâmica RF006 – M1P1


j4

46-1409 ( I) - Mus covi te-2M1, V-Ba-rich - (K,Ba,N a)0.75(Al ,M g,Cr,V)2(Si,Al,V)4O10(OH,O)2 - Y: 31.17 % - d x by: 1. - W L: 1.54056 - M onoclinic - a 5.2099 - b 9.0729 - c 20.0639 - alpha 90.000 - beta 95.715 - gam46-1045 (*) - Quartz, syn - SiO2 - Y: 31.17 % - d x by: 1. - WL: 1.54056 - Hexagonal - a 4.91344 - b 4.91344 - c 5.40524 - alpha 90.000 - beta 90.000 - gamma 120.000 - Prim itive - P3221 (154) - 3 - 113.010 - I/Ic PC:\data\ipen\casim iro\loteii\i4.R AW - Fi le: i4.R AW - Ty pe: 2Th/Th locked - Start: 3.00 ° - End: 65.00 ° - Step: 0.05 ° - Step tim e: 1. s - T emp.: 25 °C (R oom) - T im e Started: 16 s - 2-Theta: 3.00 ° - Theta: 1.50 ° - Phi:

I(cps

)

0

100 0

200 0

300 0

400 0

° (2θ)

5 10 20 30 40 50 60

p. 71

Gráfico nº 12: Difratometria de raio X da amostra de cerâmica RF006 M5R (Dr. Fábio Ramos Dias de Andrade – IGc/USP - 2007)

j5

4 6 -1 4 0 9 ( I) - M u s cov i te- 2 M 1 , V- B a- ri ch - (K ,B a,N a) 0 .7 5 ( Al ,M g ,C r ,V) 2 (S i,A l,V )4 O 1 0 (O H ,O )2 - Y: 5 5 .90 % - d x b y : 1 . - W L: 1 .5 40 5 6 - M on o c li n ic - a 5 .2 0 9 9 - b 9 .0 7 2 9 - c 2 0 .0 6 3 9 - a lp h a 9 0 .0 00 - b e ta 9 5 .7 1 5 - g a m4 6 -1 0 4 5 ( * ) - Q u a rtz , syn - S i O 2 - Y : 55 .9 0 % - d x b y : 1 . - W L : 1.5 4 0 5 6 - H e xag o n al - a 4 .91 3 4 4 - b 4 .9 1 3 4 4 - c 5 .40 5 2 4 - a lp h a 9 0 .0 00 - b e ta 9 0 .0 0 0 - g a m m a 1 2 0 .0 00 - P r im it i ve - P 3 2 2 1 (1 5 4 ) - 3 - 1 1 3 .01 0 - I /Ic PC :\d ata \i p en \ca s im ir o \l ote ii\ t5 .R A W - F ile : j 5 .R A W - T yp e: 2 T h /T h l oc ked - S tar t : 3 .0 0 ° - E nd : 6 5 .0 0 ° - S tep : 0 .05 ° - S te p t im e : 1 . s - Te m p .: 2 5 ° C (R o om ) - T im e S ta rted : 1 6 s - 2- T he ta: 3 .00 ° - T h eta : 1 .5 0 ° - Ph i :

I(cps

)

0

1 0 0 0

2 0 0 0

° ( 2 θ )

5 10 2 0 3 0 4 0 5 0 6 0

p. 72

Gráfico nº 13: Difratometria de raio X da amostra de cerâmica RF006M4R (Dr. Fábio Ramos Dias de Andrade – IGc/USP - 2007)

j6

46-1409 (I) - Muscovite-2M1, V-Ba-rich - (K,Ba,Na)0.75(Al,Mg,Cr,V)2(Si,Al,V)4O10(OH,O)2 - Y: 50.00 % - d x by: 1. - W L: 1.54056 - Monoclinic - a 5.2099 - b 9.0729 - c 20.0639 - alpha 90.000 - beta 95.715 - gam46-1045 (*) - Quartz, syn - SiO2 - Y: 50.00 % - d x by: 1. - WL: 1.54056 - Hexagonal - a 4.91344 - b 4.91344 - c 5.40524 - alpha 90.000 - beta 90.000 - gamma 120.000 - Primitive - P3221 (154) - 3 - 113.010 - I/Ic PC:\data\ipen\casimiro\loteII\t6.RAW - F ile: j6.RAW - Type: 2Th/Th locked - Start: 3.00 ° - End: 65.00 ° - Step: 0.05 ° - Step time: 1. s - Temp.: 25 °C (Room) - T ime Started: 16 s - 2-Theta: 3.00 ° - Theta: 1.50 ° - Phi:

I(cps

)

0

100 0

200 0

300 0

400 0

° (2θ)

5 10 20 30 40 50 60

p. 73


j7

46-1409 (I) - Mus covite-2M1, V-Ba-rich - (K,Ba,Na)0.75(Al,Mg,Cr,V)2(Si,Al,V)4O10(OH,O)2 - Y: 71.90 % - d x by: 1. - W L: 1.54056 - Monoclinic - a 5.2099 - b 9.0729 - c 20.0639 - alpha 90.000 - beta 95.715 - gam46-1045 (*) - Quartz, syn - SiO2 - Y: 71.90 % - d x by: 1. - WL: 1.54056 - Hexagonal - a 4.91344 - b 4.91344 - c 5.40524 - alpha 90.000 - beta 90.000 - gamma 120.000 - Pr im itive - P3221 (154) - 3 - 113.010 - I/Ic PC:\data\ipen\casimiro\loteII\t7.RAW - F ile: j7.RAW - T ype: 2Th/Th locked - Start: 3.00 ° - End: 65.00 ° - Step: 0.05 ° - Step time: 1. s - Temp.: 25 °C (Room) - T ime Started: 16 s - 2-Theta: 3.00 ° - Theta: 1.50 ° - Phi :

I(cps

)

0

100 0

200 0

300 0

° (2θ)

5 10 20 30 40 50 60

p. 74

Gráfico nº15: Difratometria de raio X da amostra de cerâmica RF006M2R (Dr. Fábio Ramos Dias de Andrade – IGc/USP - 2007)

j8

46-1409 ( I) - Mus covi te-2M1, V-Ba- ri ch - (K ,Ba,N a)0 .75 (Al ,M g,Cr ,V)2(S i,A l,V )4O 10(O H ,O)2 - Y: 48 .62 % - d x by: 1 . - W L: 1 .54056 - M onoclin ic - a 5 .2099 - b 9 .0729 - c 20 .0639 - a lpha 90 .000 - be ta 95 .715 - gam46-1045 ( *) - Qua rtz, syn - S iO2 - Y : 48 .62 % - d x by: 1 . - W L: 1.54056 - Hexagonal - a 4 .91344 - b 4 .91344 - c 5 .40524 - a lpha 90 .000 - be ta 90 .000 - gamm a 120.000 - Pr im iti ve - P3221 (154) - 3 - 113 .010 - I/Ic PC:\data \ipen \casim iro \lote II\t8 .RAW - F ile : j8 .RAW - T ype: 2Th/T h loc ked - S tar t: 3 .00 ° - End : 65 .00 ° - S tep : 0 .05 ° - S tep tim e: 1 . s - Tem p.: 25 ° C (R oom ) - T im e S tarted : 18 s - 2-T heta: 3 .00 ° - T heta : 1 .50 ° - Ph i :

I(cps

)

0

100 0

200 0

300 0

400 0

° (2θ)

5 10 20 30 40 50 60

p. 75


j9

46-1409 ( I) - Mus covi te-2M1, V-Ba-rich - (K,Ba,N a)0.75(Al ,M g,Cr,V)2(Si,A l,V)4O10(OH ,O)2 - Y: 90.25 % - d x by: 1. - W L: 1.54056 - M onoclin ic - a 5.2099 - b 9.0729 - c 20.0639 - a lpha 90.000 - beta 95.715 - gam46-1045 (*) - Quartz, syn - SiO2 - Y: 90.25 % - d x by: 1. - W L: 1.54056 - Hexagonal - a 4 .91344 - b 4.91344 - c 5.40524 - a lpha 90.000 - beta 90.000 - gamm a 120.000 - Pr im itive - P3221 (154) - 3 - 113.010 - I/Ic PC:\data\ipen\casim iro \lote ii\i9 .R AW - Fi le: j9.R AW - Ty pe: 2Th/Th locked - Star t: 3 .00 ° - End: 65.00 ° - Step: 0.05 ° - Step tim e: 1. s - T emp.: 25 °C (R oom) - T im e Star ted: 16 s - 2-Theta: 3.00 ° - Theta: 1.50 ° - Ph i:

I(cps

)

0

100 0

200 0

° (2θ)

5 10 20 30 40 50 60

p. 76

Gráfico nº 17: Difratometria de raio X da amostra de cerâmica RF006 M1D2 (Dr. Fábio Ramos Dias de Andrade – IGc/USP - 2007)

j10

46-1409 ( I) - Muscovi te-2M1, V-Ba-rich - (K,Ba,Na)0.75(Al,Mg,Cr,V)2(Si,Al,V)4O10(OH,O)2 - Y: 82.10 % - d x by: 1. - W L: 1.54056 - Monoclinic - a 5.2099 - b 9.0729 - c 20.0639 - alpha 90.000 - beta 95.715 - gam46-1045 (*) - Quartz, syn - SiO2 - Y: 82.10 % - d x by: 1. - WL: 1.54056 - Hexagonal - a 4.91344 - b 4.91344 - c 5.40524 - alpha 90.000 - beta 90.000 - gamma 120.000 - Primitive - P3221 (154) - 3 - 113.010 - I/Ic PC:\data\ipen\casim iro\loteII\t10.RAW - Fi le: j10.RAW - Type: 2Th/Th locked - Start: 3.00 ° - End: 65.00 ° - Step: 0.05 ° - Step time: 1. s - Temp.: 25 °C (Room) - T ime Started: 21 s - 2-Theta: 3.00 ° - Theta: 1.50 ° - Ph

I(cps

)

0

100 0

200 0

° (2θ)

5 10 20 30 40 50 60

p. 77

Documents

Gráfico nº 01: Difratometria de raio X da amostra de ... · 46-1409 (I) - Muscovite-2M1, V-Ba-rich - (K,Ba,Na)0.75(Al,Mg,Cr,V)2(Si,Al,V)4O10(OH,O)2 - Y: 54.84 % - d x by: 1. - WL: